EUROPEAN JOURNAL OF
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 ISSN 2394-3211

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Abstract

SYNTHESIS OF 2-[(2-PHENYLDIMINO-6-SUBSTITUTEDAMINO)-1,3,5-DITHIAZINO] IMIN-11-(PIPRAZINE-1 YL) DIBENZO[B,F][1,4] OXAZEPINES

D. T. Tayade* and P. R. Kale

ABSTRACT

Recently in this laboratory convenient method for synthesis of 2-[(2-phenylimino-6-substitutedamino)-1,3,5- dithiazino]imino-11-(piprazine-1-yl) dibenzo [b,f] [1,4] oxazepines [VIIIB(a-h)] was developed. The interactions of 2-[substituted-2,4-dithiabiureto]-11-(piperazin-1-yl)dibenzo[b,f][1,4]oxazepines [VB(a-h)] with phenylisocyanodichloride (VIIa) in 50% acetone-ethanol medium were carried out on water bath to synthesized [VB(a1-a36)] respectively. The structures of synthesized compounds were justified on the basis of chemical characteristics, elemental analysis and spectral studies.

Keywords: Phenylisothiocyanate, 2-[substituted-2,4-dithiabiureto]-11-(piperazin-1-yl) dibenzo[b,f][1,4]oxazepines and 50% acetone-ethanol.


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